Lab 10Mpa High Pressure Reactor with Magnetic Stirring for Chemical Synthesis

Characteristics and Uses:
Stainless Steel high pressure reactor autoclave is suitable for flammable, explosive, high toxic, precious media and chemical media of strong penetration to stir. It is the best no-leak response for petroleum, chemical, organic synthesis, polymer, food and other process to vulcanize, fluorate, oxidize. 
The main features of the device are static sealing structure, which can completely solve the leakage problem of stirring,keep the entire medium and mixing parts completely sealed.Therefore, it is more suitable for a variety of flammable, explosive, highly toxic, valuable media and other chemical media with strong penetration.The product integrates stirring,heating and high-pressure reaction. It is a combination of Mechanical stirrer and stainless steel high-pressure reactor for reducing the cost of research unit. The equipment is more versatile and reduce costs for user and widely used in colleges and universities, environmental protection, biochemistry, medical treatment, scientific research and other fields.

About item:
[316L Stainless Steel Construction, High-Temperature and Corrosion Resistance]: The main body is crafted from premium 316L stainless steel for stable performance. An integrated high-precision temperature probe directly monitors the core reaction temperature, ensuring a stable and reliable experimental environment.
[Explosion-Proof Safety and Pressure Monitoring]: Equipped with a stainless steel explosion-proof valve for enhanced safety. A clear, intuitive pressure gauge enables real-time, precise monitoring of pressure inside the reactor, guaranteeing operational safety.
[Fully Sealed Magnetic Stirring, Zero Leakage]: Utilizes magnetic drive stirring for complete sealing. Equipped with inlet/outlet/sampling valves to facilitate various operations and prevent medium leakage risks.
[Split-Type Quick-Release Structure with Smart Control]: The reactor body and heater separate rapidly for emergency cooling and maintenance. An integrated LCD control panel allows precise adjustment of temperature and speed with simple operation.
[Versatile Multi-Functional Reaction Platform]: Suitable for gas-liquid-solid and other multi-phase reactions, particularly for harsh media. Combining stirring, heating, and reaction functions, it serves as an ideal benchtop experimental apparatus.

Note:
Our autoclave products support capacity, temperature, pressure or material customization, if you have customization needs, please contact us! 

 

Operation Method

1. [SET] Key: Set or check temperature setpoints, speed setpoints, and internal machine parameters.

2. [TIME] Key: Set the operating time. After the set time ends, press the [HEAT] key to restart the temperature control operation.

3. [Heat] Key: Heating on/off switch.

4. [+/Toggle] Key: In non-setting mode, press and hold for 3 seconds to toggle between two temperature values and automatically save. In setting mode, press to increment the set value; press and hold to continuously increment the set value.

5. [-/Auto-Tune] Key: Press for 6 seconds in non-setting mode to enter temperature auto-tuning selection. In setting mode, press to incrementally decrease the set value; press and hold to continuously decrease the set value.

6. [SHIFT] Key: In setting mode, press to toggle, flash, and correct the set value.

7. [STIR] Key: Stirring (speed) toggle button.


 

1

Product structure

1. Stirring method: Mechanical stirring, no leakage of the shaft seal, ensuring no leakage, no exposed rotating parts, and the test is safer.

2. Stirring motor: High-power motor, powerful and stable performance.

3. Inlet gas valve: gas inlet needle valve

4. Sampling valve: It is convenient to sample and analyze the progress during the reaction.

5. Exhaust valve: It is convenient to vacuum and replace the gas before the reaction, and the reaction ends is used as a vent valve.

6. Pressure gauge: Real-time monitoring of the reaction temperature in the kettle.

7. Temperature probe: Deep into the interior of the reaction vessel and monitor the reaction temperature.

8.Heating unit: module heating, fast heating, precise control, digital display


Usage and precautions

1. When the screws are tightened, the operator must gradually apply force to tighten the screws for multiple times in a diagonal and symmetrical mode, the force must be evenly applied, and the reactor cover is not allowed to tilt to one side.

2. When tightening the main nut, do not exceed the specified tightening torque range of 40-120nm to prevent the sealing surfaces from being crushed or worn out under overload.

3. The operator should take special care of the sealing surfaces, and the upper and lower sealing surfaces should be wiped clean with a piece of gentle paper or cloth before each installation.

4. Do not form scars on the sealing surfaces of the reactor body and the reactor cover. If the sealing surfaces are damaged, they needs to be reprocessed and repaired to achieve good sealing performance.

5. When the reactor cover is disassembled, it should be slowly lifted and it is strictly prohibited to disassemble the reactor cover under pressure. After the reaction is completed, the reactor body should cool down naturally to the room temperature and then can be opened. The sealing surfaces between the reactor body and the reactor cover are prevented from colliding with each other.

6. It is recommended that the external heating temperature should not exceed 200 degrees Celsius in the working process, and the heating rate should be less than or equal to 5 ℃ min.

7. The filling degree of the interior of the reactor should not exceed 80%.

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