Lab Hydrothermal Synthesis Reactor Stainless Steel Autoclav Reactor PTFE Chamber
[Basic parameters] PTFE Liner Max temperature: 200 ℃, Security temperature: 180 ℃, Max pressure: 4MPa, Security pressure: 3MPa,Heating/Cooling Rate: 5 C/min
[Liner] The PTFE liner has no dead angle, high lubricity and non-stickiness, high temperature resistance, high pressure resistance, corrosion resistance, physical inertness and almost insoluble in all solvents.
[Kettle body - safety] The stainless steel body is integrally processed and formed, the 304 stainless steel wall is thickened, and the refined thread is matched with the lengthened tightening rod to create a high-pressure air-tight reaction environment to ensure safe experiments.
[Air tightness] The kettle lid body and seal are made of durable and reliable cable sealing structure, and the sealing effect is stable and leak-free for a long time.
[lab Usage] It is helpful for dissolving samples in the determination of trace elements. It can be used for the determination of copper, cadmium, zinc, calcium, manganese, iron, mercury and other heavy metals, and can also be used as a high-purity high-pressure high-temperature corrosion-resistant reaction vessel. It can also be used in inorganic synthesis, hydrothermal synthesis, crystal growth, digestion and extraction, etc.


WHAT IS A HYDROTHERMAL SYNTHESIS AUTOCLAVE REACTOE?

The Hydrothermal Autoclave reactor use to carry hydrothermal reaction at high pressure and high temperature, which adopts the external heating mode, is a kind of closed container to dissolve the refractory material .

There generally comes in a two variety: Polytetrafluoroethylene (PTFE) lined & PPL lined autoclave. Hydrothermal reactor mainly made up of two parts: outer stainless steel shell and inner PTFE liner or PPL chamber. In the Teflon-lined autoclave, the reaction is carried out at maximum 220-degree Celsius (428 Fahrenheit), while the safe temperature is 180-degree Celsius (356 Fahrenheit). PPL lined reactor use for the reaction operate at higher temperature, where the safe temperature will be 250-degree Celsius (482 Fahrenheit) and the maximum operating temperature is 280-degree Celsius (536 Fahrenheit). This product is widely used in catalysis, crystal, polymer and other experiments.

It could be used to pretreat the samples in atomic absorption spectrometry and plasma emission analysis, etc.

Also, it is suitable for small dose synthetic reaction, to rapidly dissolve the refractory material under the reactor inner strong acid or strong base and high temperature & high pressure airtight environment.

Our Teflon Lined Hydrothermal Synthesis Autoclave is widely used in new materials, energy, environmental engineering and other fields of scientific research and experiments, it is a small commonly used reactor used in teaching and scientific research.

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  • Fashion Appearance & Reasonable Structure: Stainless steel sheel, beautiful appearance, strong & durable. High safety, , easy operation.
  • SS304 high quality stainless steel reactor body. Use circular groove sealing, manual spiral firm, excellent sealing performance.
  • PTFE lining. Ultra Strong Corrosion Resistant Performance. Dissolve Sample Rapidly Without Any Lossless. The solution should preferably not exceed 80%
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OPERATING GUIDE

  1. Place the Autoclave and sterilizing material on the table.
  2. Release the screw type threaded primary SS cap in an anticlockwise direction until it has been opened.
  3. Lift the top lid and take-out the reaction chamber.
  4. Fill solvent (as per liner's capacity) in the reaction chamber and sealed it. Make sure that the cap should be air-tight to avoid pressure leakage.
  5. Place the liner in a stainless steel chamber.
  6. Keep top gasket over the vessel and make sure that the vessel placed properly in the Stainless Steel chamber.
  7. Then twist primary SS cap in a clockwise direction until it does not turn anymore.
  8. The secondary SS cap has been given at the top of the primary cap for extra tightening to avoid pressure leakages.
  9. Rotate primary SS cap in the clockwise direction with the help of locking rod for additional tightening.
  10. Placed the hydrothermal autoclave in oven or furnace and heat it till reactor’s safe temperature.
  11. Increase the temperature of the oven and set heating rate 5℃/minute only.
  12. A researcher can heat the hydrothermal autoclave till 180℃ for safe use.
  13. After completion of the hydrothermal synthesis reaction, the autoclave's cooling rate will be 5℃/minute.
  14. Make sure that, after completion of the process clean the liner properly for reuse.
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